Record Details

Development of a laser interferometric dilatometer

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Field Value
Title Development of a laser interferometric dilatometer
Names Johnson, Phillip Merle (creator)
Johnson, Linwood E. (advisor)
Date Issued 1964-09-02 (iso8601)
Note Graduation date: 1965
Abstract Thermal expansion is one of the most frequently measured
physical properties of materials. One of the important methods
of detecting and measuring these changes is dilatometry, which
is measuring the thermal expansion of the specimen and relating
the specimen's expansion to its temperature.
Four major types of dilatometers are commonly used:
The precision micrometric method, the Fizeau-Pulfrich interferometric
dilatometer, the quartz tube and dial indicator
apparatus, and the autographic optical lever method. These
methods have various shortcomings and are not particularly
suited for high temperature application.
The development of the laser, which provided a high
intensity monochromatic light source, prompted the investigation of interferometric configurations as a dilatometer technique. The
interferometer has distinct advantages over other systems in that
the measurement is absolute, that is, calibration is not needed as
measurements are made directly in terms of a wavelength of
light and are relatively contactless in nature.
The purpose of this investigation was to determine the
feasibility of a dilatometer using an interferometric configuration
with a gas laser light source and to construct a working model
interferometers characteristically break a light beam into two
wave trains which, when reunited, will interfere if a phase shift
has occurred. The dilatometer configuration developed suspends
the specimen in the center of a one inch by eight inch long
tantalum heating element such that the specimen is contained in
one of the beams of the interferometer, As the specimen changes
length, the path containing the specimen changes length, causing
a change in the point of interference. The interference bands are
counted as they pass in front of a photoconductive cell orifice.
The only direct contact between the specimen and the dilatometer
is at the supporting wires.
The feasibility of using an interferometric configuration
utilizing the polished ends of the specimen has been demonstrated
by various experiments, one of which was to produce fringes at
1,000°C using a polished steel specimen. Various experiments using a Michelson interferometer and a gas laser produced clear,
stable fringes which could be easily counted. Preliminary measurements
have been made to 500°F with the dilatometer.
The specimen and support system were heated to 1,000°C
for one hour. The performance of the vacuum system and the
cooling system was satisfactory. Subsequent inspection of the
support system, etc., showed that it was undamaged. Calculations
indicate an upper limit of the present configuration with the
particular laser light source to be about 1,800°C. Preliminary
data indicate the accuracy of the apparatus to be about five per
cent compared to a probable accuracy for an improved model of
about two per cent.
The dilatometer measurement errors can be grouped in
optical errors, errors due to differential thermal expansion in
the apparatus, and readout errors. Most of the errors are
independent of the coefficient of expansion of the specimen; thus,
the percentage error will be largely determined by the coefficient
of thermal expansion of the material measured. All of the errors
except the errors due to the movement of the specimen and its
support system can be reduced or eliminated by proper design
and use of materials which have low coefficients of thermal
expansion. Movement of the specimen causes a series of second
order errors, estimated in the aggregate to be less than twenty millionths of an inch per 100°C.
The use of the gas laser light source in an interferometric
configuration for dilatometry is feasible and has definite high
temperature potential. A working model has been built and some
preliminary measurement capability demonstrated.
Genre Thesis/Dissertation
Topic Dilatometer
Identifier http://hdl.handle.net/1957/48594

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