Record Details
Field | Value |
---|---|
Title | Condensation reactions of certain aldehydes and amines with acetylbenzoyl |
Names |
Klemm, Waldemar Arthur, Jr.
(creator) Logan, A. V. (advisor) |
Date Issued | 1967-05-05 (iso8601) |
Note | Graduation date: 1967 |
Abstract | Acetylbenzoyl reacted with dimethylamine hydrochloride and benzaldehyde in primary isoamyl alcohol under reflux conditions to form 1,4-diphenvl-3-butene-1,2-dione, compound I, which melted at 56-57°C. Compound I formed a quinoxaline derivative, compound II, which melted at 152.5-153°C. Compound I was cleaved by hydrogen peroxide to form cinnamic acid, compound III, which melted at 133°C. Acetylbenzoyl reacted with dimethylamine hydrochloride and benzaldehyde in glacial acetic acid under reflux conditions to form 1,4,5-tripheny-1,2,5-pentanetrione, compound IV, which melted at 192-193°C, Compound IV formed an oxime derivative, compound V, which melted at 232-233°C. |
Genre | Thesis/Dissertation |
Topic | Acetylbenzoyl |
Identifier | http://hdl.handle.net/1957/47467 |